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lines changed Original file line number Diff line number Diff line change @@ -11642,6 +11642,7 @@ save_PD_QPA_INTERNAL_STD
1164211642
1164311643 _description_example.case
1164411644;
11645+ _audit.schema Custom
1164511646 _pd_diffractogram.id DIFFRACTOGRAM_1
1164611647
1164711648 loop_
@@ -11663,14 +11664,14 @@ save_PD_QPA_INTERNAL_STD
1166311664 _description_example.detail
1166411665;
1166511666 A diffraction pattern containing three phases (PHASE_1, PHASE_2, and
11666- some NIST SRM646a ) has been quantified using the ZMV algorithm after
11667+ some NIST SRM676a ) has been quantified using the ZMV algorithm after
1166711668 Rietveld refinement.
1166811669
1166911670 The diffraction pattern was collected from a specimen containing
1167011671 25.000 ± 0.002 wt% internal standard (i.e. 1 g added to 3 g of unknown
1167111672 to make a specimen with total weight of 4 g). The internal standard is
1167211673 known to be 99.02 ± 1.11 % crystalline, and so the reported value of
11673- _pd_phase_mass.percent for the standard is 25.000 * 0.9902 = 24.96 wt%.
11674+ _pd_phase_mass.absolute for the standard is 25.000 * 0.9902 = 24.76 wt%.
1167411675
1167511676 The weight fractions derived from the ZMW algorithm were then scaled as
1167611677
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