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cif_pow.dic

Lines changed: 3 additions & 2 deletions
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@@ -11642,6 +11642,7 @@ save_PD_QPA_INTERNAL_STD
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_description_example.case
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;
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_audit.schema Custom
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_pd_diffractogram.id DIFFRACTOGRAM_1
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loop_
@@ -11663,14 +11664,14 @@ save_PD_QPA_INTERNAL_STD
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_description_example.detail
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;
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A diffraction pattern containing three phases (PHASE_1, PHASE_2, and
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some NIST SRM646a) has been quantified using the ZMV algorithm after
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some NIST SRM676a) has been quantified using the ZMV algorithm after
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Rietveld refinement.
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The diffraction pattern was collected from a specimen containing
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25.000 ± 0.002 wt% internal standard (i.e. 1 g added to 3 g of unknown
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to make a specimen with total weight of 4 g). The internal standard is
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known to be 99.02 ± 1.11 % crystalline, and so the reported value of
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_pd_phase_mass.percent for the standard is 25.000 * 0.9902 = 24.96 wt%.
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_pd_phase_mass.absolute for the standard is 25.000 * 0.9902 = 24.76 wt%.
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The weight fractions derived from the ZMW algorithm were then scaled as
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