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We performed high-temperature (900–1200°C), high-pressure (\~5 GPa), and high-stress forced-oscillation experiments on polycrystalline olivine in a multi-anvil apparatus called a deformation-DIA. In these experiments we applied a sinusoidal force to our samples. We then used the bright X-rays produced by the APS to measure the deformation (also referred to as ‘strain’) of our samples from digital image correlation of radiographs. We measured the stress that the rock experienced by diffracting X-rays through the crystal lattice of the sample and converting the elastic lattice strains to stresses using Hooke’s law. The time delay between the imposed sinusoidal stress and the measured sinusoidal strain is directly related to a quantity known as the inverse quality factor, *Q*\-1, that is commonly used by seismologists to quantify the attenuation of seismic waves traveling through the mantle after earthquakes. By changing the stress amplitude of the imposed oscillations we were able to observe that *Q*\-1 increased with amplitude (Figure 1), which is diagnostic of attenuation produced by dislocations.
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To confirm that the trend we observed could not be attributed to changes in grain size or crystallographic orientations over the course of our experiments, we characterized the microstructure of our samples before and after deformation by electron backscatter diffraction using a scanning electron microscope. These analyses confirmed that the evolution of grain size and crystallographic orientations could not explain our observations. Therefore, our measurements of *Q*\-1 provide a first-of-its-kind dataset to compare to the predictions of the plastic-anisotropy and backstress models.
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Because there are no analytical solutions to the constitutive equations of these models, we performed numerical simulations of our experiments, solving the equations for the strain produced by a sinusoidally varying stress. Figure 2 presents a comparison of the attenuation from our experiments to the attenuation predicted by the plastic-anisotropy and backstress models. The comparison clearly illustrates that the plastic-anisotropy model underpredicts the amount of attenuation observed in our experiments, especially at lower temperatures. As such, we conclude that the plastic-anisotropy of olivine did not dominate the behavior of the olivine in our experiments.
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, and predictions of the backstress and plastic anisotropy models (solid and dotted lines, respectively) at a period (*p*) of 300 s. Colors refer to temperatures and shaded areas represent the approximate error of experimental results due to the temperature-uncertainty in the deformation-DIA apparatus.")
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, and predictions of the backstress and plastic anisotropy models (solid and dotted lines, respectively) at a period (*p*) of 300 s. Colors refer to temperatures and shaded areas represent the approximate error of experimental results due to the temperature-uncertainty in the deformation-DIA apparatus.")
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 is the tectonic background stress, \\(\sigma_{\mathrm{A}}\\) is the amplitude of the seismic wave, increasing temperature is indicated by colors of increasing warmth, \\(\omega\\) is frequency). Seismological constraints on attenuation in upper oceanic mantle (PREM, NoMelt) are plotted for comparison, as well as an extrapolation of the recent recalibration of a popular grain-boundary sliding model (dashed lines).")
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 is the tectonic background stress, \\(\sigma_{\mathrm{A}}\\) is the amplitude of the seismic wave, increasing temperature is indicated by colors of increasing warmth, \\(\omega\\) is frequency). Seismological constraints on attenuation in upper oceanic mantle (PREM, NoMelt) are plotted for comparison, as well as an extrapolation of the recent recalibration of a popular grain-boundary sliding model (dashed lines).")
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